Crystals of para-quaterphenyl and its trimethylsilyl derivative. I. Growth from solutions, structure and crystal chemical analysis by the Hirschfeld surface method

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Abstract

The results of crystal growth of para-quaterphenyl (4P) and its derivative – 4,4''-bis(trimethylsilyl)-para-quaterphenyl (TMS-4P-TMS) from solutions are presented. It has been established that TMS-4P-TMS crystals exhibit better growth characteristics compared to 4P. Parameters of phase transitions of 4P and TMS-4P-TMS in closed crucibles were refined using the method of differential scanning calorimetry. The crystal structure of TMS-4P-TMS in the triclinic space group P1 (Z = 2) has been decrypted for the first time using single-crystal X-ray diffraction and studied over a wide temperature range. Crystallographic analysis of the studied compounds in crystals was performed using the Hirshfeld surface method, and modeling of intermolecular interactions was conducted.

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V. A. Postnikov

Shubnikov Institute of Crystallography of Kurchatov Complex of Crystallography and Photonics of NRC “Kurchatov Institute”

Author for correspondence.
Email: postva@yandex.ru
Russian Federation, Moscow

N. I. Sorokina

Shubnikov Institute of Crystallography of Kurchatov Complex of Crystallography and Photonics of NRC “Kurchatov Institute”

Email: postva@yandex.ru
Russian Federation, Moscow

M. S. Lyasnikova

Shubnikov Institute of Crystallography of Kurchatov Complex of Crystallography and Photonics of NRC “Kurchatov Institute”

Email: lyasnikova.m@crys.ras.ru
Russian Federation, Moscow

G. A. Yurasik

Shubnikov Institute of Crystallography of Kurchatov Complex of Crystallography and Photonics of NRC “Kurchatov Institute”

Email: postva@yandex.ru
Russian Federation, Moscow

A. A. Kylishov

Shubnikov Institute of Crystallography of Kurchatov Complex of Crystallography and Photonics of NRC “Kurchatov Institute”

Email: postva@yandex.ru
Russian Federation, Moscow

T. A. Sorokin

Shubnikov Institute of Crystallography of Kurchatov Complex of Crystallography and Photonics of NRC “Kurchatov Institute”

Email: postva@yandex.ru
Russian Federation, Moscow

O. V. Borshchev

Enikolopov Institute of Synthetic Polymer Materials of Russian Academy of Sciences

Email: postva@yandex.ru
Russian Federation, Moscow

E. A. Svidchenko

Enikolopov Institute of Synthetic Polymer Materials of Russian Academy of Sciences

Email: postva@yandex.ru
Russian Federation, Moscow

N. M. Surin

Enikolopov Institute of Synthetic Polymer Materials of Russian Academy of Sciences

Email: postva@yandex.ru
Russian Federation, Moscow

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